AOAC 20th Ed 2016 List of Changes

Ofcial Methods of Analysis 20th Edition (2016) Front Maer

Standard Method Performance Requirements (SMPRs®): AOAC SMPR® 2011.009 Standard Method Performance Requirements for Requirements for Cr, Mo, and Se in Infant Formula and Adult/Pediatric Nutrional Formula

Revised January 2015 to correct Ta Table ble 1, footnote b, to read: “µg/kg reconstuted nal product” AOAC SMPR® 2011.011 Standard Method Performance Requirements for Requirements for in vi tro Determinaon of Total Anoxidant Acvity in Foods, Beverages, Food Ingredients, and Dietary Supplements

Approved by AOAC Stakeholder Panel on Strategic Foods Analycal Method (SPSF (SPSFAM) AM) and revised March 2013 to not require establishing equivalency of results NEW AOAC SMPR® 2012.001 Standard Method Performance Requirements for Requirements for Flavanols in Foods and

Beverages NEW AOAC SMPR® 2012.002 Standard Method Performance Requirements for Requirements for Whey Protein:Casein Rao

in Infant Formula NEW AOAC SMPR® 2012.003 Standard Method Performance Requirements for Requirements for Vitamin A in Preblends,

Premixes, and Pure Materials NEW AOAC SMPR® 2012.004 Standard Method Performance Requirements for Requirements for Vitamin D in Preblends,

Premixes, and Pure Materials NEW AOAC SMPR® 2012.005 Standard Method Performance Requirements for Requirements for Vitamin E in Preblends,

Premixes, and Pure Materials NEW AOAC SMPR® 2012.006 Standard Method Performance Requirements for Requirements for Vitamin K in Preblends,

Premixes, and Pure Materials NEW AOAC SMPR® 2012.007 Standard Method Performance Requirements for Requirements for Heavy Metals in a Variety

of Foods and Beverages NEW AOAC SMPR® 2012.008 Standard Method Performance Requirements for Requirements for Iodine in Infant Formula

and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2012.009 Standard Method Performance Requirements for Requirements for Pantothenic Acid in Infant

Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2012.010 Standard Method Performance Requirements for Requirements for L-Carnine in Infant

Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2012.011 Standard Method Performance Requirements for Requirements for Fay Acids, Including

LCPUFAs, LCPUF As, in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2012.012 Standard Method Performance Requirements for Requirements for Vitamin C in Infant Formula

and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2012.013 Standard Method Performance Requirements for Requirements for Total Choline in Infant

Formula and Adult Pediatric Nutrional Formula NEW AOAC SMPR® 2013.001 Standard Method Performance Requirements for Requirements for Hypericins, Hyperforins,

and Flavonoids in St. John’s Wort (Hypericum (Hypericum perforatum) perforatum) and Other Hypericum Hypericum spp. spp. NEW AOAC SMPR® 2014.001 Standard Method Performance Requirements for Requirements for Vitamin K in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2014.002 Standard Method Performance Requirements for Requirements for Fructans in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2014.003 Standard Method Performance Requirements for Requirements for Galactooligosaccharides (GOS) in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2014.004 Standard Method Performance Requirements for Requirements for Minerals and Trace Elements in Infant Formula and Adult/Pediatric Nutrional Formula

If you have any questions of a technical nature or suggestions for editorial changes, please e-mail us at [email protected].

iii

© 2016 AOAC INTERNATIONAL

NEW AOAC SMPR® 2014.005 Standard Method Performance Requirements for Bion in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR ® 2014.006 Standard Method Performance Requirements for Detecon and Idencaon of Variola Virus in Aerosol Collecon Filters and/or Liquids NEW AOAC SMPR® 2014.007 Standard Method Performance Requirements for Authencaon of Selected Vaccinium species (Anthocyanins) in Dietary Ingredients and Dietary Supplements NEW AOAC SMPR® 2014.008 Standard Method Performance Requirements for Screening Method for Selected Adulterants in Dietary Ingredients and Supplements Containing Chondroin Sulfate NEW AOAC SMPR® 2014.009 Standard Method Performance Requirements for Total Chondroin Sulfate in Dietary Ingredients and Supplements NEW AOAC SMPR® 2014.010 Standard Method Performance Requirements for Idencaon of Phosphodiesterase Type 5 (PDE5) Inhibitors in Dietary Ingredients and Supplements NEW AOAC SMPR® 2014.011 Standard Method Performance Requirements for Quantave Methods for

Determinaon of Phosphodiesterase Type 5 (PDE5) Inhibitors in Dietary Ingredients and Supplements NEW AOAC SMPR® 2014.012 Standard Method Performance Requirements for Screening Methods for Phosphodiesterase Type 5 (PDE5) Inhibitors in Dietary Ingredients and Supplements NEW AOAC SMPR® 2014.013 Standard Method Performance Requirements for Amino Acids in Infant and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2014.014 Standard Method Performance Requirements for Selected Carotenoids in Infant and Adult/ Pediatric Nutrional Formula NEW AOAC SMPR® 2014.015 Standard Method Performance Requirements for Chloride in Infant and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2014.016 Standard Method Performance Requirements for Fluoride in Infant and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2014.017 Standard Method Performance Requirements for Detecon of Salmonella species in Romaine Leuce and Baby Spinach NEW AOAC SMPR® 2015.001 Standard Method Performance Requirements for Sodium Fluoroacetate

(“Compound 1080”) in Infant Formula NEW AOAC SMPR® 2015.002 Standard Method Performance Requirements for Total Vitamin B1 (Thiamine) in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2015.003 Standard Method Performance Requirements for Total Vitamin B2 (Riboavin) in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2015.004 Standard Method Performance Requirements for Total Vitamin B3 (Niacin) in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2015.005 Standard Method Performance Requirements for Total Vitamin B6 (Pyridoxine) in Infant Formula and Adult/Pediatric Nutrional Formula NEW AOAC SMPR® 2015.006 Standard Method Performance Requirements for Quantaon of Arsenic Species in Selected Foods and Beverages NEW AOAC SMPR® 2015.007 Standard Method Performance Requirements for Withanolide Glycosides and Aglycones of Ashwagandha (Withania somnifera) NEW AOAC SMPR® 2015.008 Standard Method Performance Requirements for Alkaloids of Mitragyna

speciosa NEW AOAC SMPR® 2015.009 Standard Method Performance Requirements for Esmaon of Total Phenolic Content Using the Folin-C Assay NEW AOAC SMPR® 2015.010 Standard Method Performance Requirements for Idencaon of Selected Cinnamomum spp. Bark in Dietary Supplement Raw Materials and/or Finished Products NEW AOAC SMPR® 2015.011 Standard Method Performance Requirements for Detecon of Coxiella

burnei NEW AOAC SMPR® 2015.012 Standard Method Performance Requirements for Idencaon of

Venezuelan Equine Encephalis Virus NEW AOAC SMPR® 2015.013 Standard Method Performance Requirements for Detecon of Staphylococcal

enterotoxin B NEW AOAC SMPR® 2015.014 Standard Method Performance Requirements for Determinaon of Catechins, Methyl Xanthines, Theaavins, and Theanines in Tea Dietary Ingredients and Supplements


iv

NEW AOAC SMPR® 2015.015 Standard Method Performance Requirements for Aloin A and Aloin B in Dietary Supplement Products and Ingredients NEW AOAC SMPR® 2015.016 Standard Method Performance Requirements for Vitamin D in Dietary Finished Products and Ingredients

Chapter 2

942.02 (2.6.29) Zinc in Ferlizers

Included full text 942.03 (2.6.30) Zinc in Ferlizers

Included full text Chapter 4

971.09 (4.4.04) Pepsin Digesbility of Animal Protein Feeds

Updated October 2012: B(a): Deleted “Agitator and boles available from Terry Sims (1901 Laurel Rd, Oceanside, CA 92054, USA, Tel: +1-760-722-4119).” NEW 2014.10 (4.7.07) Dietary Starch in Animal Feeds and Pet Food NEW 2012.25 (4.10.07) Residues of Three Triphenylmethane Dyes and Their Metabolites (Malachite Green,

Leucomalachite Green, Crystal Violet, Leucocrystal Violet, and Brill iant Green) in Aquaculture Product Final Acon 2016: Approved by the Ocial Methods Board in February 2016 Chapter 5

2008.01 (5.2.07) Lasalocid Sodium in Animal Feeds and Premixes

Final Acon 2013 2008.08 (5.3.25) Decoquinate in Animal Feeds

Final Acon 2013 2008.09 (5.3.26) Oxytetracycline/Oxytetracycline Hydrochloride in Animal Feed, Fish Feed, and Animal

Remedies Final Acon 2013 Chapter 6

955.14 (6.2.01) Tesng Disinfectants Against Salmonella enterica

Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised March 2013 to include editorial and procedural revisions 955.15 (6.2.04) Tesng Disinfectants Against Staphylococcus aureus

Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised March 2013 to include editorial and procedural revisions Revised September 2013 to include editorial and procedural revisions: C(f ): Deleted “Maximum diluon of germicide which kills test organism on 10 carriers in 10 min interval

represents presumed maximum safe use diluon for praccal disinfecon.” and “Note: While killing in 10 of 10 replicates specied provides reasonably reliable index in most cases, killing in 59 of 60 replicates is necessary for condence level of 95%.” Included new secon C(h) on Performance Standard and Note 964.02 (6.2.06) Tesng Disinfectants Against Pseudomonas aeruginosa

Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised March 2013 to include editorial and procedural revisions Revised September 2013 to include editorial and procedural revisions: C(f ): Deleted “Maximum diluon of germicide which kills test organism on 10 carriers in 10 min interval

represents presumed maximum safe use diluon for praccal disinfecon.” and “Note: While killing in 10 of 10 replicates specied provides reasonably reliable index in most cases, killing in 59 of 60 replicates is necessary for condence level of 95%.” Included new secon C(h) on Performance Standard and Note 960.09 (6.3.03) Germicidal and Detergent Sanizing Acon of Disinfectants

Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised March 2013 to include editorial and procedural revisions 961.02 (6.3.04) Germicidal Spray Products as Disinfectants

Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised March 2013 to include editorial and procedural revisions 966.04 (6.3.05) Sporicidal Acvity of Disinfectants

Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised March 2013 to include editorial and procedural revisions

v


965.12 (6.3.06) Tuberculocidal Acvity of Disinfectants

Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised December 2012 to include editorial and procedural revisions 2008.05 (6.3.09) Ecacy of Liquid Sporicides Against Spores of Bacillus sublis on Hard Nonporous and

Porous Surfaces Approved by Methods Commiee on Anmicrobial Ecacy Tesng and revised March 2013 to include editorial and procedural revisions Chapter 7

2011.26 (7.8.12) Phenols and Phenates in Disinfectant Formulaons

Final Acon 2013 Moved from Chapter 6 (6.1.04) to Chapter 7 (7.8.12) Revised December 2012 to correct conversion factors in Table 2011.26E Chapter 9

NEW 2013.06 (9.1.10) Arsenic, Cadmium, Mercury, and Lead in Foods NEW 2015.01 (9.2.42) Heavy Metals in Food

Chapter 10

2007.01 (10.1.04) Pescide Residues in Foods by Acetonitrile Extracon and Paroning with Magnesium

Sulfate Final Acon 2013 2010.03 (10.6.32) Bifenthrin i n Technical and Selected Formulated Products

Final Acon 2013 2007.08 (10.7.05) Low-Level Pescide Residues in So Drinks and Sports Drinks

Final Acon 2013 2007.09 (10.7.06) Pescide Residues (>0.5 μg/L) in So Drinks and Sports Drinks

Final Acon 2013 Chapter 11

973.51 (11.1.14) Chloride in Water

Revised January 2015 to read: B(a) ... “Dissolve 824.1 mg NaCl, previously dried at 140°C for 2 h and cooled in a desiccator, in Cl-free H2O and dilute to 1 L.” ... Chapter 16

972.40 (16.14.23) Light Filth in Pepper

Revised January 2015 to correct cross reference for sieve Chapter 17

NEW 2014.05 (17.2.11) Enumeraon of Yeast and Mold in Food NEW 2015.13 (17.2.12) Enumeraon of Aerobic Bacteria in Food 996.10 (17.4.01B) Transia ® AG EHEC for the Detecon of Escherichia coli O157:H7 in Selected Foods

Approved by Methods Commiee on Microbiology and revised December 2015 to indicate new test kit name and addional minor editorial revisions 2005.04 (17.4.01E) Escherichia coli O157:H7 in Selected Foods

Approved by Methods Commiee on Microbiology and revised December 2012 to add an increased test poron size (375 g) 2005.05 (17.4.06A) Shigatoxin genes, from E. coli O157:H7, in Selected Foods

Approved by Methods Commiee on Microbiology and revised December 2012 to add an increased test poron size (375 g) 2000.14 (17.4.07) Reveal for E. coli O157:H7 Test in Selected Foods and Environmental Swabs

Table 2000.14B: Corrected table numbering 999.08 (17.9.25) Transia ® AG Salmonella EIA for the Visual or Instrumental Detecon of Mole and

Nonmole Salmonella in All Foods Approved by Methods Commiee on Microbiology and revised December 2015 to indicate new test kit name and addional minor editorial revisions 2009.03 (17.9.35) Salmonella in Foods and Environmental Surfaces

Revised First Acon 2015: Approved by ERP in March 2015 for matrix extension NEW 2013.01 (17.9.36) Salmonella in a Variety of Foods

Final Acon 2016: : Approved by the Ocial Methods Board in February 2016 NEW 2013.02 (17.9.37) Salmonella Species in a Variety of Foods and Environmental Surfaces

Final Acon 2016: : Approved by the Ocial Methods Board in February 2016


vi

NEW 2013.09 (17.9.38) Salmonella in Selected Foods

Revised First Acon 2014 Final Acon 2016: : Approved by the Ocial Methods Board in February 2016 NEW 2013.14 (17.9.39) Idencaon of Salmonella spp. from Colony Picks

Final Acon 2016: : Approved by the Ocial Methods Board in February 2016 NEW 2014.01 (17.9.40) Salmonella in Selected Foods

996.14 (17.10.07) Transia ® AG Listeria for the Detecon of Listeria monocytogenes and Related Listeria

Species in Selected Foods and Environmental Surfaces Approved by Methods Commiee on Microbiology and revised December 2015 to indicate new test kit name and addional minor editorial revisions NEW 2013.10 (17.10.14) Listeria Species in a Variety of Foods and Environmental Surfaces

Final Acon 2016: : Approved by the Ocial Methods Board in February 2016 NEW 2013.11 (17.10.15) Listeria monocytogenes in a Variety of Foods

Final Acon 2016: : Approved by the Ocial Methods Board in February 2016 NEW 2014.06 (17.10.16) Listeria species in Selected Foods and Environmental Surfaces NEW 2014.07 (17.10.17) Listeria monocytogenes in Selected Foods and Environmental Surfaces NEW 2012.06 (17.14.06) Bacillus anthracis in Aerosol Collecon Samples 2012.02 (17.15.02) Gram-Posive Bacteria Idencaon

Included reference: “ J. AOAC Int . 95, 1425(2012)” Final Acon 2016: : Approved by the Ocial Methods Board in February 2016 NEW 2013.08 (17.16.01) Ricin Powder on Nonporous Surfaces

Chapter 23

2011.23 (23.1.19) Determinaon and Conrmaon of Parent and Total Ractopamine in Bovine, Swine, and

Turkey Tissues Final Acon 2012: Revised to reect Final Acon status and included reference to Final Acon paper [ J. AOAC Int . 96, 917(2013)] 2011.24 (23.1.20) Determinaon and Conrmaon of Narasin and Monensin in Chicken, Swine and B ovine

Tissues Final Acon 2012: Revised to reect Final Acon status and included reference to Final Acon paper [ J. AOAC Int . 96, 902(2013)] NEW 2013.07 (23.1.21) Determinaon and Conrmaon of Nicarbazin in Chicken Tissues

Chapter 28

NEW 2013.12 (28.1.49) Total Carbohydrates in Wine and Wine-Like Beverages

Chapter 30

NEW 2014.09 (30.1.35) High-Throughput Analycal Techniques for Determinaon and Conrmaon of

Residues of 653 Mul-Class Pescides and Chemical Pollutants in Tea Chapter 31

NEW 2012.24 (31.5.14) Flavanol and Procyanidin (by Degree of Polymerizaon 1-10) Content of Chocolate,

Cocoa Liquors, Powder(s), and Cocoa Flavanol Extracts NEW 2013.03 (31.5.15) Analysis of Cocoa Flavanols and Procyanidins (DP 1-10) in Cocoa-Containing

Ingredients and Products NEW 2013.04 (31.5.16) Catechin and Epicatechin Enanomers in Cocoa-Based Ingredients and Products

Chapter 32

NEW 2014.03 (32.1.45) Gluten in Rice Flour and Rice-Based Food Products NEW 2015.05 (32.2.11) Parally Hydrolyzed Gluten in Fermented Cereal-Based Products

Chapter 33

2006.06 (33.2.67) Lactose in Milk

Final Acon 2013 920.119 (33.6.11) Color Addives in Buerfat

General Test secon: Revised July 2014 to reference Chapter 46 on Color Addives, not Chapter 34 Chapter 35

977.13 (35.1.32) Histamine in Seafood

Revised November 2012: C(b): 79.33 mL (not 73.33 mL) 85% (15 M H3PO4) NEW 2014.08 (35.1.46) Polycyclic Aromac Hydrocarbons (PAHs) in Seafood

Chapter 36

2006.05 (36.2.24) Site-Specic Deuterium/Hydrogen (D/H) Raos in Vanillin

Final Acon 2013

vii


Chapter 39

972.22 (39.1.13) Phosphorus in Meat

Include full text 970.42 (39.1.17) Nitrogen in Meat

Include full text 2008.06 (39.1.39) Moisture and Fat in Meats


998.12 (44.4.18A) C-4 Plant Sugars in Honey

Revised First Acon 2013: Modicaon approved by Ocial Methods Board in January 2013 to add ltraon and/or centrifugaon Deleted parenthecal text below tle: “(Method is used...concentraon >7%)” Replaced stascal performance data with Table 998.12 A: Added the following sentence: “Addion of C-4 sugars (cane sugar/corn syrup) to honey increases the

value of the stable carbon isotope rao of the honey.” A: Replaced “is a measure” with “allows for the detecon and an esmate of the amount” Protein, C: Replaced last sentence “Product is considered to contain signicant C-4 sugars (primarily corn

or cane) only at or above 7%.” to “Pure honey (free of corn or cane sugars), with an excepon of a few unusual variees, yields a value of C-4 sugars of ≤7%. Some unusual variees may slightly exceed the range, but will have δ13C for honey which are in the normal range (more negave than –24.0‰).” Included reference to modicaon: “ J. AOAC Int . 96, 607(2013)” Chapter 45

997.08 (45.4.06A) Fructans in Food Products

Revised April 2013: C(e): Included availability of Fructanase liquid 994.10 (45.4.10) Cholesterol in Foods

Revised November 2014: C(b): Replaced “Hexamethyldisilane (HMDS).—CAS No. 1450-14-2” with “Hexamethyldisilazane (HMDS).—CAS No. 999-97-3” Chapter 47

2012.03 (47.2.05) Anoxidant Capacity of Commercial Beverages

Included reference: “ J. AOAC Int . 95, 1558(2012)” 2012.04 (47.2.06) Anoxidant Acvity in Foods and Beverages

Included reference: “ J. AOAC Int . 95, 1562(2012)” NEW 2012.23 (47.2.07) Total Anoxidant Acvity

Chapter 49

2008.02 (49.2.32) Aatoxins B1, B2, G1, and G2 and Ochratoxin A in Ginseng and Ginger

Final Acon 2013 NEW 2013.05 (49.3.08) Aatoxins B1, B2, G1, and G2 in Olive Oil, Peanut Oil, and Sesame Oil 2011.02 (49.10.05) Paralyc Shellsh Toxins in Mussels, Clams, Oysters, and Scallops


2011.05 (50.1.28) Folate in Infant Formula and Adult/Pediatric

Repealed 2014 2011.06 (50.1.29) Total Folates in Infant Formula and Adult Nutrionals

Revised as follows: A: Six (not seven) folate vitamers are quaned and the total folates determined and expressed as folic

acid D(a)(2): 4.8 mL (not 5 g) glacial acec acid D(b)(2): 4.8 mL (not 0.5 g) glacial acec acid

Table 2011.06F: Included tle “Formula weight” Included reference: “ J. AOAC Int . 95, 1547(2012)” 2011.08 (50.1.31) Vitamin B12 in Infant Formula and Adult Nutrionals

Repealed 2014 2011.10 (50.1.33) Vitamin B12 in Infant and Pediatric Formulas and Adult Nutrionals

Final Acon 2014: Approved by Ocial Methods Board in November 2014 ISO-AOAC Method


viii

2011.12 (50.1.35) Vitamins D2 and D3 in Infant Formula and Adult Nutrionals

Repealed 2014 2011.13 (50.1.36) Vitamins D2 and D3 in Infant Formula and Adult Nutrionals

Repealed 2014 2011.14 (50.1.37) Calcium, Copper, Iron, Magnesium, Manganese, Potassium, Phosphorus, Sodium, and

Zinc in Fored Food Products Final Acon 2013 2011.15 (50.1.38) Vitamin A (Renol) in Infant Formula and Adult Nutrionals

Repealed 2014 2011.16 (50.1.39) Vitamin B12 in Infant Formula and Adult Nutrionals

Repealed 2014 2011.18 (50.1.40) Myo-Inositol (Free and Bound as Phosphadylinositol) in Infant Formula and Adult

Nutrionals Final Acon 2014: Approved by Ocial Methods Board in November 2014 ISO-AOAC Method 2011.19 (50.1.41) Chromium, Selenium, and Molybdenum in Infant Formula and Adult Nutrional Products

Final Acon 2014: Approved by Ocial Methods Board in November 2014 ISO/IDF-AOAC Method 2011.20 (50.1.42) 5 -Mononucleodes in Infant Formula and Adult/Pediatric Nutrional Formula ′

Final Acon 2014: Approved by Ocial Methods Board in November 2014 ISO-AOAC Method NEW 2012.26 (50.1.44) Bovine Immunoglobulin G in Bovine Colostrum Powders, Bovine Milk Powders, and

Dietary Supplements Containing Bovine Colostrum Products NEW 2012.09 (50.2.01) Simultaneous Determinaon of Vitamins A and E in Infant Formula and Adult/

Pediatric Nutrional Formula NEW 2012.10 (50.2.02) Simultaneous Determinaon of Vitamins E and A in Infant Formula and Adult

Nutrionals Final Acon 2014: Approved by Ocial Methods Board in November 2014 ISO-AOAC Method NEW 2012.11 (50.2.03) Simultaneous Determinaon of Vitamins D2 and D3 in Infant Formula and Adult/

Pediatric Nutrional Formula

NEW 2012.16 (50.2.04) Pantothenic Acid (Vitamin B5) in Infant Formula and Adult/Pediatric Nutrional

Formula

Final Acon 2015: Approved by Ocial Methods Board in July 2015 ISO-AOAC Method NEW 2012.21 (50.2.05) Vitamin C in Infant Formula and Adult/Pediatric Nutrional Formula NEW 2014.02 (50.2.06) Vitamin B12 in Infant Formula and Adult/Pediatric Formulas NEW 2012.22 (50.2.07) Vitamin C in Infant Formula and Adult/Pediatric Nutrional Formula

Revised November 2013: D(a), D(d), and G(a)(6): Corrected concentraons of mobile phase NEW 2015.09 (50.2.08) Vitamin K1 in Infant, Pediatric, and Adult Nutrionals NEW 2012.13 (50.3.01) Labeled Fay Acids Content in Milk Products and Infant Formulae and Adult

Pediatric Nutrional Formula Final Acon 2014: Approved by Ocial Methods Board in November 2014 ISO/IDF-AOAC Method NEW 2013.13 (50.4.01) Folate in Infant Formula and Adult/Pediatric Nutrional Formula NEW 2012.07 (50.5.01) Calculaon of Whey Protein in Milk-Based Infant Formula NEW 2012.08 (50.5.02) Whey Protein Content in Milk-Based Infant Formula Finished Products

Revised April 2015 to correct Equaon 7 NEW 2012.17 (50.6.01) Free and Total Carnine in Infant Formula and Adult/Pediatric Nutrional Formula

ix


NEW 2012.18 (50.6.02) Choline in Infant Formula and Adult/Pediatric Nutrional Formula NEW 2012.20 (50.6.03) Choline in Infant Formula and Adult Nutrionals NEW 2014.04 (50.6.04) Simultaneous Determinaon of Choline/Carnine in Infant Formulas and Adult

Nutrional Products NEW 2015.10 (50.6.05) Free and Total Choline and Carnine in Infant Formula and Adult/Pediatric

Nutrional Formula NEW 2012.12 (50.7.01) Free and Total Myo-Inositol in Infant Formula and Adult/Pediatric Nutrional

Formula NEW 2012.14 (50.8.01) Total Iodine in Infant Formula and Nutrional Products NEW 2012.15 (50.8.02) Total Iodine in Infant Formula and Adult/Pediatric Nutrional Formula

Final Acon 2015: Approved by Ocial Methods Board in July 2015 ISO/IDF-AOAC Method NEW 2015.02 (50.9.01) Sodium Monouoroacetate in Dairy Powders NEW 2015.03 (50.9.02) Sodium Fluoroacetate in Infant Formula NEW 2015.04 (50.9.03) Monouoroacetate in Powdered Nutrional Products NEW 2015.06 (50.10.01) Minerals and Trace Elements in Infant Formula and Adult/Pediatric Nutrional

Formula NEW 2015.07 (50.11.01) Chloride in Infant Formula and Adult/Pediatric Nutrional Formula NEW 2015.08 (50.11.02) Chloride in Infant Formula and Adult Nutrionals NEW Subchapter on AOAC SPIFAN Final Acon Ocial MethodsSM with Joint Organizaonal Approvals

(along with their respecve SMPRs) Chapter 51

2007.03 (51.5.01) Campesterol, Sgmasterol, and Beta-Sitosterol in Saw Palmeo Raw Materials and

Dietary Supplements Final Acon 2013 2007.05 (51.6.01) Aristolochic Acid I in Botanicals and Dietary Supplements Potenally Contaminated with

Aristolochic Acid I Final Acon 2013 NEW 2015.11 (51.10.01) Chondroin Sulfate Content in Raw Materials and Dietary Supplements NEW 2015.12 (51.11.01) Screening and Idencaon of Phosphodiesterase Type 5 Inhibitors in Dietary

Ingredients and Supplements Appendix G

Procedures and Guidelines for the Use of AOAC Voluntary Consensus Standards to Evaluate Characteriscs of a Method of Analysis

Revised February 2014 to include the denion of a quorum under the seconGuidance Documents, Expert Review Panels, item (3) Appendix K

Guidelines for Dietary Supplements and Botanicals Revised October 2013 to correct Horwitz equaon in secon 3.4.2

Appendix N

NEW ISPAM Guidelines for Validaon of Qualitave Binary Chemistry Methods

Subject Index

Revised to reect changes in the 20th Edion

SMPR Index

NEW

Index of Method Numbers

Revised to reect changes in the 20th Edion


x

AOAC 20th Ed 2016 List of Changes

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